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Organic Chemistry
- Are borneol and isoborneol considered diastereomers or enantiomers? Why?
- Why can one mole of borohydride reduce four moles of camphor (consider structure)?
- Why is the endo or exo attack of the hydride on the camphor the preferred approach?
- What is being reduced and what is being oxidized in the reduction of camphor to isoborneol? How can you tell?
- Why did the isoborneol precipitate out of solution when the "ice water" was added?
- What was the one main purpose for dissolving the precipitated isoborneol in methylene chloride, adding drying agent, and then distilling off the methylene chloride?
- See Pavia, Part C, NMR Determination to answer the following questions.
- At which chemical shift does the hydrogen on the carbon bearing the hydroxyl group appear in the proton NMR spectra of:
- Borneol 1 point
- Isoborneol 1 point
- Given the 1H-NMR spectral data resulting from a student's Reduction of Camphor experiment (below), calculate what percent of the student's product was Borneol and what percent was Isoborneol. Show all work.
- At which chemical shift does the hydrogen on the carbon bearing the hydroxyl group appear in the proton NMR spectra of:
Shift (ppm)
Integration
4.0
1.05
3.6
6.24
- See Pavia, Part C, NMR Determination to answer the following questions.