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Compound 2 is a volatile liquid (boiling point 88 'C). The Mass, IR, and 1H NMR spectra, along with ”C NMR data, are givenbelow; the molecular ion, (m/e = 102) does not show in the mass spectrum. Elemental Analysis: C, 58.80; H, 9.87; 0, 31.33. Mass SpectrumM Intensny N30 4D 50 60 70 80 90 100 110 120 130 1‘0 150 160 170 1a) 150 200 m/eInfrared Spectrum Wave Number, cm -1N— 4000 3000 2500 2000 1500 130012001100 1000 900 000 700 ”C Spectral Data: singlet, 171.0 ppm Mdoublet, 68.3 ppm quartet, 23.0 ppm K‘s—Rquartet, 17.6 ppm W

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